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NancyLebovitz comments on What are some science mistakes you made in college? - Less Wrong Discussion
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http://www.buzzfeed.com/kmallikarjuna/how-to-science-as-told-by-17-overly-honest-scientists
I'm not sure how much of this is mistakes, exactly, but it's definitely about sub-optimal experiments. Sometimes way sub-optimal.
Drawback: there is no way to verify this material.